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. 2015 Jun 17;71(Pt 7):810–812. doi: 10.1107/S2056989015010798

Table 2. Experimental details.

Crystal data
Chemical formula (C6H10N3O3)[AuCl4]
M r 510.94
Crystal system, space group Monoclinic, P21/n
Temperature (K) 130
a, b, c () 7.324(2), 11.972(4), 15.667(5)
() 94.384(4)
V (3) 1369.6(8)
Z 4
Radiation type Mo K
(mm1) 11.52
Crystal size (mm) 0.23 0.04 0.02
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2013)
T min, T max 0.426, 0.746
No. of measured, independent and observed [I > 2(I)] reflections 22024, 4214, 3673
R int 0.041
(sin /)max (1) 0.718
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.021, 0.045, 1.16
No. of reflections 4214
No. of parameters 163
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
max, min (e 3) 1.30, 1.22

Computer programs: APEX2 and, SAINT (Bruker, 2013), SHELXS97 and SHELXTL (Sheldrick, 2008), SHELXL2014 (Sheldrick, 2015).