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. 2015 Jun 17;71(Pt 7):799–806. doi: 10.1107/S2056989015011354

Table 1. Comparison of the XO (X = Mo, W) and NaO bond lengths () in Na2MoO42D2O and Na2WO42D2O with those of the protonated isotopologues reported in the literature.

  Na2MoO42D2O Na2MoO42H2O Na2WO42D2O Na2WO42H2O
  This work Capitelli et al. (2006) This work Farrugia (2007)
XO1 1.773(2) 1.772(1) 1.785(2) 1.776(3)
XO2 1.764(1) 1.767(1) 1.778(2) 1.778(3)
XO3 1.750(2) 1.751(1) 1.766(2) 1.761(3)
XO4 1.776(2) 1.778(1) 1.783(2) 1.787(3)
Mean XO 1.766 1.767 1.778 1.776
         
Na1O2 2.437(3) 2.446(2) 2.433(2) 2.442(3)
Na1O2(i) 2.417(3) 2.419(2) 2.412(3) 2.416(3)
Na1O3(ii) 2.482(3) 2.481(2) 2.479(3) 2.480(3)
Na1O4(iii) 2.410(3) 2.395(2) 2.399(2) 2.388(3)
Na1O5 2.476(3) 2.456(2) 2.479(3) 2.464(4)
Na1O6 2.426(3) 2.423(2) 2.443(3) 2.433(3)
Mean Na1O 2.441 2.437 2.441 2.437
         
Na2O1iv 2.312(3) 2.319(2) 2.320(2) 2.323(3)
Na2O2 2.363(3) 2.354(2) 2.355(2) 2.346(3)
Na2O3v 2.339(3) 2.341(2) 2.328(2) 2.331(3)
Na2O5 2.415(3) 2.403(2) 2.409(3) 2.396(3)
Na2O6vi 2.305(3) 2.300(2) 2.311(2) 2.304(3)
Mean Na2O 2.347 2.343 2.345 2.340

Symmetry codes: (i) 1x, 1y, 1z; (ii) Inline graphic+x, Inline graphic y, 1z; (iii) Inline graphic x, Inline graphic+y, z; (iv) Inline graphic+x, Inline graphic y, 1z; (v) Inline graphic x, Inline graphic+y, z; (vi) Inline graphic+x, y, Inline graphic z.