Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C15H15N3S2 |
| M r | 301.44 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c () | 8.1035(4), 12.0193(5), 15.1312(7) |
| () | 94.347(2) |
| V (3) | 1469.52(12) |
| Z | 4 |
| Radiation type | Cu K |
| (mm1) | 3.22 |
| Crystal size (mm) | 0.27 0.25 0.24 |
| Data collection | |
| Diffractometer | Bruker X8 Proteum |
| Absorption correction | Multi-scan (SADABS; Bruker, 2013 ▸) |
| T min, T max | 0.477, 0.512 |
| No. of measured, independent and observed [I > 2(I)] reflections | 11926, 2397, 2262 |
| R int | 0.044 |
| (sin /)max (1) | 0.583 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.046, 0.127, 1.07 |
| No. of reflections | 2397 |
| No. of parameters | 183 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.37, 0.44 |