Bruker SMART APEXII CCD diffractometer | 1269 reflections with I > 2σ(I) |
Radiation source: fine focus sealed tube | Rint = 0.019 |
ω scans | θmax = 26.4°, θmin = 3.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −10→10 |
Tmin = 0.930, Tmax = 0.991 | k = −10→10 |
9178 measured reflections | l = −20→20 |
1289 independent reflections |