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. 2015 May 20;4(3):212–223. doi: 10.1002/open.201500018

Table 3.

Effects of different residence times in the CF DIBALH reduction of ethyl hydrocinnamate (Figure 1).24

Entry Volume of R A1 Residence time Selectivity for
[μL] [mL min−1] [s] aldehyde ester alcohol
1 23 5 0.23 36 64 0
2 23 10 0.11 50 50 0
3 23 30 0.04 96 4 0
4 228 5 2.28 43 57 0
5 228 10 1.14 61 39 0
6 228 30 0.38 97 3 0
7 684 5 6.84 57 43 0
8 684 10 3.42 85 15 0
9 684 30 1.14 96 3 1