Table 4.
Precision and accuracy of 2-DG HPLC assay in plasma (within-run n=3; between-run n=4)
| 2-DG conc. (μg/ml) norminal | Measured (μg/mL) Mean ± SD |
Precision (% R.S.D) | Accuracy (% norminal) | |||
|---|---|---|---|---|---|---|
|
| ||||||
| Intraday | Interday | Intraday | Interday | Intraday | Interday | |
| 0.63 | 0.68±0.03 | 0.69±0.07 | 3.9 | 9.8 | 108.1 | 110.0 |
| 2.5 | 2.2±0.2 | 2.5±0.1 | 9.8 | 3.3 | 86.8 | 98.9 |
| 10.0 | 9.7±0.3 | 9.5±0.2 | 2.8 | 1.9 | 96.9 | 95.1 |
| 50.0 | 49.6±1.0 | 49.9±1.7 | 2.0 | 3.4 | 99.3 | 99.8 |