Table 3. Data collection and processing.
Values in parentheses are for the outer shell.
| Diffraction source | BM14, ESRF |
| Wavelength () | 0.9762 |
| Temperature (K) | 100 |
| Detector | MAR225 |
| Crystal-to-detector distance (mm) | 232.09 |
| Rotation range per image () | 0.5 |
| Total rotation range () | 62.5 |
| Exposure time per image (s) | 3 |
| Space group | I422 |
| Unit-cell parameters () | a = b = 133.85, c = 75.08 |
| Mean I half-set correlation CC1/2 | 0.99 (0.54) |
| Mosaicity () | 0.73 |
| Resolution range () | 66.932.16 (2.282.16) |
| Total No. of reflections | 91937 (12661) |
| No. of unique reflections | 18347 (2640) |
| Completeness (%) | 99.4 (99.9) |
| Multiplicity | 5.0 (4.8) |
| I/(I) | 13.1 (1.4) |
| R meas | 0.062 (1.152) |
| Overall B factor from Wilson plot (2) | 56.5 |