Table 1.
1 b | 2 b | |
---|---|---|
position | δC,type | δC,type |
2 | 157.80,C | 157.79,C |
3 | 135.11,C | 135.12,C |
4 | 178.77,C | 178.77,C |
5 | 160.98,C | 160.99,C |
6 | 98.59,CH | 98.60,CH |
7 | 161.88,C | 161.89,C |
8 | 108.77,C | 108.78,C |
9 | 153.48,C | 153.49,C |
10 | 106.06,C | 106.07,C |
11 | 21.89,CH2 | 21.90,CH2 |
12 | 122.60,CH | 122.61,CH |
13 | 131.58,C | 131.58,C |
14 | 25.94,CH3 | 25.93,CH3 |
15 | 18.33,CH3 | 18.33,CH3 |
1' | 122.73,C | 122.74,C |
2',6' | 131.04,CH | 131.04,CH |
3',5' | 114.55,CH | 114.56,CH |
4' | 159.56,C | 159.56,C |
1'' | 102.46,CH | 102.46,CH |
2'' | 70.12,CH | 70.13,CH |
3'' | 70.55,CH | 70.55,CH |
4'' | 71.18,CH | 71.17,CH |
5'' | 70.78,CH | 70.79,CH |
6'' | 17.93,CH3 | 17.93,CH3 |
1''' | 101.01,CH | 101.01,CH |
2''' | 73.83,CH | 73.84,CH |
3''' | 77.07,CH | 77.08,CH |
4''' | 71.58,CH | 71.85,CH |
5''' | 77.66,CH | 77.67,CH |
6''' | 61.10,CH2 | 70.17,CH2 |
OCH3 | 55.98,CH3 | 55.99,CH3 |
aThe chemical shifts (δ) are expressed in parts per million. bData recorded in dimethyl sulfoxide-d6