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. Author manuscript; available in PMC: 2016 Sep 1.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2015 Jul 17;1000:105–111. doi: 10.1016/j.jchromb.2015.07.018

Table 3.

Stability results for ManNAc and Neu5Ac in LQC (5% BSA) and in HQC (human plasma).

ManNAc LQC (30.0 ng/mL) HQC (4051 ng/mL)
Deviation (%) Deviation (%)
Room temperature for 16 h 8.4 −7.8
Freeze/thaw 4 cycles 1.1 0.3
Autosampler at 2–8 °C for 48 h 8.5 −4.7
Processed sample at 2–8 °C for 48 h 0.0 −1.6
Long-term at −80 °C for 310 days 2.2 2.4
Neu5Ac LQC (75.0 ng/mL) HQC (8159 ng/mL)
Deviation (%) Deviation (%)
Room temperature for 16 h −0.6 −6.2
Freeze/thaw 4 cycles 0.2 −5.8
Autosampler at 2–8 °C for 96 h −1.6 1.8
Processed sample at 2–8 °C for 48 h 10.1 −11.1
Long-term −80 °C for 309 days 3.6 −5.8