Table 1. Data collection and refinement statistics.
| AnAPN1 | |
|---|---|
| Data collection | |
| Space group | P212121 |
| Cell dimensions | |
| a, b, c (Å) | 113.48, 132.9, 146.01 |
| α β γ (°) | 90.0, 90.0, 90.0 |
| Resolution (Å) | 98.0-2.65 (2.72-2.65)a |
| Rmerge | 0.111 (0.842) |
| I / σI | 13.5 (2.3) |
| Completeness (%) | 99.5 (99.2) |
| Redundancy | 8.8 (8.0) |
| Refinement | |
| Resolution (Å) | 64.0 -2.65 |
| No. reflections | 61048 |
| Rwork / Rfree | 20.3/25.4 |
| No. atoms | |
| Protein | 14067 |
| Ligand/ion | 96 |
| Water | 146 |
| B factors | |
| Protein | 59.5 |
| Ligand/ion | 69.5 |
| Water | 49.7 |
| r.m.s. deviations | |
| Bond lengths (Å) | 0.0120 |
| Bond angles (°) | 1.52 |
a
Values in parentheses are for highest-resolution shell.
Data was collected from a single crystal.