Table 1. Description of the data-collection parameters for the XRPD experiments.

Space group	X-ray source	Beamline	Detector	Resolution ()	Capillary diameter (mm)	No. of exposures per position	Exposure time per scan	No. of scans
P21()	Synchrotron radiation	ID31, ESRF	APD†	6.5	1.0	2	2min	6
		MS-X04SA, SLS	Mythen‡	6.5	0.5	35	2s	12
P21()	Synchrotron radiation	ID31, ESRF	APD	12	1.0	2	2min	6
C2	Synchrotron radiation	ID31, ESRF	APD	7	1.0	2	2min	6
		MS-X04SA, SLS	Mythen	9	0.5	35	2s	12
P21()	Synchrotron radiation	ID31, ESRF	APD	6	1.0	2	2min	6
		MS-X04SA, SLS	Mythen	9	0.5	35	2s	12

^†Nine Si(111) analyser crystals each followed by a point detector [avalanche photodiode (APD) detectors].

^‡Modular (each module covering 5 in 2) one-dimensional solid-state Si microstrip detector (Mythen II) covering 120 in 2.