Table 1.
S.no. | Compounds | Column solvent | Yield (mg) | Melting point (°C) | Optical rotation (c, 0.02, MeOH) |
---|---|---|---|---|---|
1 | Cyclo(D-Leu-D-Arg) | 30% DCM in hexane | 19 | 202.51−205.55 | [a]D − 118 |
2 | Cyclo(L-Trp-L-Arg) | 75% DCM in hexane | 16 | 265.1−267.34 | [a]D + 145 |
3 | Cyclo(D-Trp-D-Arg) | 15% ethyl acetate in DCM | 21 | 262.23−265.58 | [a]D − 167 |