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. 2014 Nov 12;50(2):493–518. doi: 10.1007/s10853-014-8685-2

Table 16.

SEM/SDD-EDS analysis of fluorides (results in atom fractions); 7 replicates

Fluoride F ideal F mean Relative error (%) σ Relative σ (%) Metal ideal Metal mean Relative error (%) σ Relative σ (%)
NaF 0.5000 0.5143 2.9 0.00069 0.13 0.5000 0.4857 −2.9 0.00069 0.14
CaF2 0.6667 0.6686 0.29 0.00074 0.11 0.3333 0.3314 −0.57 0.00074 0.22
SrF2 0.6667 0.6611 −0.83 0.00021 0.032 0.3333 0.3389 1.7 0.00021 0.062
BaF2 0.6667 0.6527 −2.1 0.00152 0.23 0.3333 0.3473 4.2 0.00152 0.44
LaF3 0.7500 0.7600 1.3 0.00283 0.37 0.2500 0.2400 −4.0 0.00283 1.2