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. 2015 Aug 29;71(Pt 9):1109–1113. doi: 10.1107/S2056989015015649

Table 2. Experimental details.

Crystal data
Chemical formula CaIrO3
M r 280.30
Crystal system, space group Orthorhombic, C m c m
Temperature (K) 298
a, b, c () 3.1466(5), 9.8690(16), 7.3019(5)
V (3) 226.75(6)
Z 4
Radiation type Mo K
(mm1) 61.02
Crystal size (mm) 0.20 0.01 0.01
 
Data collection
Diffractometer Rigaku AFC7R
Absorption correction scan (North et al., 1968)
T min, T max 0.486, 0.543
No. of measured, independent and observed [F > 3.0(F)] reflections 2593, 692, 438
R int 0.019
(sin /)max (1) 1.078
 
Refinement
R[F > 3(F 2)], wR(F), S 0.011, 0.010, 1.56
No. of reflections 412
No. of parameters 20
max, min (e 3) 1.21, 1.89

Computer programs: WinAFC (Rigaku, 1999), RADY (Sasaki, 1987), ATOMS for Windows (Dowty, 2000) and publCIF (Westrip, 2010).