Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [FeCl2(C14H30N4)]PF6 |
| M r | 526.14 |
| Crystal system, space group | Orthorhombic, P n a21 |
| Temperature (K) | 150 |
| a, b, c () | 26.002(4), 8.5752(15), 9.3829(16) |
| V (3) | 2092.1(6) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 1.11 |
| Crystal size (mm) | 0.12 0.09 0.07 |
| Data collection | |
| Diffractometer | Stoe IPDS2 |
| No. of measured, independent and observed [I > 2(I)] reflections | 21858, 4186, 2249 |
| R int | 0.143 |
| (sin /)max (1) | 0.620 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.050, 0.109, 0.84 |
| No. of reflections | 4186 |
| No. of parameters | 254 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.39, 0.33 |
| Absolute structure | Refined as a two-component inversion twin |
| Absolute structure parameter | 0.03(5) |