| Crystal data |
| Chemical formula |
[RuCl(C10H8N2)(C30H20N6)]PF6
|
|
M
r
|
902.19 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
120 |
|
a, b, c () |
8.678(4), 13.743(7), 18.999(10) |
| , , () |
94.913(7), 90.583(7), 91.316(7) |
|
V (3) |
2257(2) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.50 |
| Crystal size (mm) |
0.20 0.12 0.08 |
| |
| Data collection |
| Diffractometer |
Bruker D8 with APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2007 ▸) |
|
T
min, T
max
|
0.703, 0.961 |
| No. of measured, independent and observed [I > 2(I)] reflections |
22054, 8243, 4937 |
|
R
int
|
0.109 |
| (sin /)max (1) |
0.604 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.062, 0.136, 0.91 |
| No. of reflections |
8243 |
| No. of parameters |
578 |
| No. of restraints |
48 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.74, 0.74 |
