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. 2015 Aug 22;71(Pt 9):1058–1060. doi: 10.1107/S2056989015015315

Table 2. Experimental details.

Crystal data
Chemical formula [Ag(C13H11N3)2]NO3
M r 588.37
Crystal system, space group Orthorhombic, P b c n
Temperature (K) 296
a, b, c () 11.9903(2), 10.1377(2), 20.1115(5)
V (3) 2444.63(9)
Z 4
Radiation type Mo K
(mm1) 0.87
Crystal size (mm) 0.18 0.16 0.15
 
Data collection
Diffractometer Bruker SMART CCD area detector
Absorption correction Multi-scan (SADABS; Bruker, 2002)
T min, T max 0.846, 0.872
No. of measured, independent and observed [I > 2(I)] reflections 62591, 3043, 2446
R int 0.034
(sin /)max (1) 0.667
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.030, 0.080, 1.06
No. of reflections 3043
No. of parameters 182
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
max, min (e 3) 0.44, 0.48

Computer programs: SMART and SAINT (Bruker, 2002), SHELXS2013 (Sheldrick, 2008), SHELXL2013 (Sheldrick, 2015), ORTEP-3 for Windows (Farrugia, 2012) and publCIF (Westrip, 2010).