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. 2015 Aug 15;71(Pt 9):o659–o660. doi: 10.1107/S2056989015014395
Bruker APEXII CCD diffractometer 2686 independent reflections
Radiation source: fine-focus sealed tube 2164 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.027
ω and φ scans θmax = 26.4°, θmin = 2.3°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −11→12
Tmin = 0.652, Tmax = 0.746 k = −15→15
21437 measured reflections l = −14→12