Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.025	Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.063	H-atom parameters constrained
S = 1.13	w = 1/[σ2(Fo2) + (0.0315P)2 + 3.4263P] where P = (Fo2 + 2Fc2)/3
5564 reflections	(Δ/σ)max = 0.003
345 parameters	Δρmax = 0.98 e Å−3
0 restraints	Δρmin = −0.92 e Å−3