| Crystal data |
| Chemical formula |
[CoFe(C5H5)(C16H14N2O2)(C11H9N2O)] |
|
M
r
|
631.36 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
10.684(2), 11.989(3), 13.858(3) |
| , , () |
80.220(5), 85.234(5), 80.047(5) |
|
V (3) |
1720.2(7) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.94 |
| Crystal size (mm) |
0.2 0.2 0.1 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEXII area detector |
| Absorption correction |
Multi-scan (SADABS; Sheldrick, 2012 ▸) |
|
T
min, T
max
|
0.639, 0.745 |
| No. of measured, independent and observed [I > 2(I)] reflections |
10667, 7295, 3968 |
|
R
int
|
0.047 |
| (sin /)max (1) |
0.644 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.056, 0.136, 0.93 |
| No. of reflections |
7295 |
| No. of parameters |
521 |
| No. of restraints |
638 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.62, 0.58 |
