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. 2015 Aug 25;71(Pt 9):1200–1204. doi: 10.1107/S2053230X15014375

Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source Beamline BL14.1, BESSY II
Wavelength () 0.91841
Temperature (K) 100
Detector PILATUS 6M
Crystal-to-detector distance (mm) 345
Rotation range per image () 0.1
Total rotation range () 140
Exposure time per image (s) 15
Space group P21
Unit-cell parameters (, ) a = 74.64, b = 94.72, c = 117.40, = = 90, = 90.672
Mosaicity () 0.276
Resolution range () 50.02.0 (2.12.0)
Total No. of reflections 411089 (57278)
No. of unique reflections 110108 (14992)
Completeness (%) 99.5 (99.9)
Multiplicity 3.73 (3.82)
I/(I) 9.09 (2.37)
R r.i.m. 0.114 (0.669)
Overall B factor from Wilson plot (2) 31.39