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. Author manuscript; available in PMC: 2015 Sep 4.
Published in final edited form as: Anal Methods. 2014 Feb 25;6(8):2592–2607. doi: 10.1039/C3AY42085J

Table 3.

Recoveries of OPA vapor spikes from S10 LpDNPH samplers after storage at room temperaturea

Quantity of OPA
vapor collected (µg)
Period of
storage (days)
Quantity of OPA
found (µg)
Recovery
0.71 3 0.68 95.8%
0.71 6 0.66 93.0%
0.71 10 0.61 85.9%
0.71 15 0.69 96.8%
5.17 3 5.15 99.6%
5.17 6 4.99 97.1%
5.17 10 5.24 101.3%
5.17 15 4.85 93.8%
14.5 3 14.4 99.3%
14.5 6 13.5 93.1%
14.5 10 12.2 84.1%
14.5 15 10.9 75.2%
a

Aliquots of acetonitrile solutions of OPA were deposited on PTFE-GFFs, and pumps operated at 1.0 L min−1 in a nitrogen atmosphere.