Skip to main content
. Author manuscript; available in PMC: 2015 Sep 4.
Published in final edited form as: Anal Methods. 2014 Feb 25;6(8):2592–2607. doi: 10.1039/C3AY42085J

Table 4.

Recoveries of OPA vapor following air draw through S10 LpDNPH samplersa

Quantity of OPA
vapor collected (µg)
Period of air draw through
DNPH sampler @ 1.0 L min−1 (min)
Average quantity
of OPA found (µg)
Average recoveryb RSD
0.86 240 0.731 0.850 0.060
1.16 15 1.21 1.039 0.0284
1.32 120 1.12 0.850 0.0319
1.25 369 0.785 0.628 0.157
6.49 15 6.53 1.003 0.0382
6.16 120 5.80 0.942 0.0322
6.24 363 4.18 0.670 0.364
19.2 15 16.1 0.836 0.179
18.0 120 15.9 0.881 0.0407
18.9 360 17.1 0.904 0.0830
a

Aliquots of acetonitrile solutions of OPA were deposited onto PTFE-GFFs, and pumps operated at 1.0 L min−1 in a nitrogen atmosphere.

b

Each average recovery was based on four samples. Thus, Table 4 represents 40 samples.