Bruker SMART CCD area-detector diffractometer | 8477 independent reflections |
Radiation source: fine-focus sealed tube | 7744 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.030 |
phi and ω scans | θmax = 65.0°, θmin = 2.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2002) | h = −13→13 |
Tmin = 0.806, Tmax = 0.806 | k = −12→15 |
18595 measured reflections | l = −42→38 |