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. 2015 Jul 15;71(Pt 8):o576–o577. doi: 10.1107/S2056989015012335
C1—O7 1.431 (3) C29—H29 1.0000
C1—C2 1.530 (3) C30—C31 1.532 (3)
C1—C11 1.549 (3) C30—H30A 0.9900
C1—H1 1.0000 C30—H30B 0.9900
C2—C3 1.512 (4) C31—C32 1.534 (3)
C2—H2A 0.9900 C31—C41 1.556 (3)
C2—H2B 0.9900 C31—H31 1.0000
C3—C4 1.504 (3) C32—O11 1.450 (3)
C3—H3A 0.9900 C32—C39 1.546 (3)
C3—H3B 0.9900 C32—C33 1.576 (3)
C4—O2 1.467 (3) C33—O14 1.419 (3)
C4—C5 1.538 (3) C33—C38 1.526 (3)
C4—C18 1.539 (3) C33—C34 1.554 (3)
C5—C6 1.548 (3) C34—C36 1.564 (3)
C5—C11 1.552 (3) C34—C35 1.566 (3)
C5—H5 1.0000 C34—H34 1.0000
C6—C7 1.534 (3) C35—C41 1.535 (3)
C6—H6A 0.9900 C36—C37 1.543 (3)
C6—H6B 0.9900 C36—H36A 0.9900
C7—C8 1.532 (3) C36—H36B 0.9900
C7—C17 1.544 (3) C37—C38 1.514 (3)
C7—H7 1.0000 C37—C40 1.536 (3)
C8—O4 1.441 (3) C37—H37 1.0000
C8—C15 1.546 (3) C38—O12 1.429 (3)
C8—C9 1.569 (3) C38—H38 1.0000
C9—O3 1.421 (3) C39—C40 1.536 (3)
C9—C14 1.511 (3) C39—H39A 0.9900
C9—C10 1.551 (3) C39—H39B 0.9900
C10—C12 1.565 (3) C40—O13 1.432 (3)
C10—C11 1.565 (3) C40—H40 1.0000
C10—H10 1.0000 C41—N4 1.470 (3)
C11—C17 1.536 (3) C41—H41 1.0000
C12—C13 1.543 (4) C42—N4 1.466 (3)
C12—H12A 0.9900 C42—H42A 0.9900
C12—H12B 0.9900 C42—H42B 0.9900
C13—C14 1.513 (4) C43—O8 1.218 (3)
C13—C16 1.530 (4) C43—O9 1.346 (3)
C13—H13 1.0000 C43—C1'' 1.467 (3)
C14—O5 1.427 (3) C44—O10 1.425 (3)
C14—H14 1.0000 C44—H44A 0.9800
C15—C16 1.526 (4) C44—H44B 0.9800
C15—H15A 0.9900 C44—H44C 0.9800
C15—H15B 0.9900 C45—O12 1.415 (3)
C16—O6 1.429 (3) C45—H45A 0.9800
C16—H16 1.0000 C45—H45B 0.9800
C17—N2 1.474 (3) C45—H45C 0.9800
C17—H17 1.0000 C46—O13 1.411 (3)
C18—N2 1.462 (3) C46—H46A 0.9800
C18—H18A 0.9900 C46—H46B 0.9800
C18—H18B 0.9900 C46—H46C 0.9800
C19—O1 1.217 (3) C47—N4 1.459 (3)
C19—O2 1.343 (3) C47—C48 1.507 (4)
C19—C1' 1.478 (4) C47—H47A 0.9900
C20—O7 1.409 (4) C47—H47B 0.9900
C20—H20A 0.9800 C48—H48A 0.9800
C20—H20B 0.9800 C48—H48B 0.9800
C20—H20C 0.9800 C48—H48C 0.9800
C21—O6 1.419 (4) C1'—C6' 1.390 (4)
C21—H21A 0.9800 C1'—C2' 1.408 (4)
C21—H21B 0.9800 C2'—N1 1.368 (4)
C21—H21C 0.9800 C2'—C3' 1.395 (5)
C22—O5 1.403 (3) C3'—C4' 1.364 (6)
C22—H22A 0.9800 C3'—H3' 0.9500
C22—H22B 0.9800 C4'—C5' 1.366 (5)
C22—H22C 0.9800 C4'—H4' 0.9500
C23—N2 1.460 (3) C5'—C6' 1.363 (5)
C23—C24 1.508 (4) C5'—H5' 0.9500
C23—H23A 0.9900 C6'—H6' 0.9500
C23—H23B 0.9900 C1''—C6'' 1.405 (3)
C24—H24A 0.9800 C1''—C2'' 1.406 (3)
C24—H24B 0.9800 C2''—N3 1.375 (4)
C24—H24C 0.9800 C2''—C3'' 1.400 (4)
C25—O10 1.421 (3) C3''—C4'' 1.372 (4)
C25—C26 1.535 (3) C3''—H3'' 0.9500
C25—C35 1.555 (3) C4''—C5'' 1.372 (4)
C25—H25 1.0000 C4''—H4'' 0.9500
C26—C27 1.508 (3) C5''—C6'' 1.357 (3)
C26—H26A 0.9900 C5''—H5'' 0.9500
C26—H26B 0.9900 C6''—H6'' 0.9500
C27—C28 1.519 (3) N1—H1A 0.9100
C27—H27A 0.9900 N1—H1B 0.9100
C27—H27B 0.9900 N3—H3C 0.9100
C28—O9 1.467 (2) N3—H3D 0.9100
C28—C29 1.528 (3) O3—H3 0.8400
C28—C42 1.543 (3) O4—H4 0.8400
C29—C30 1.551 (3) O11—H11 0.8400
C29—C35 1.555 (3) O14—H14A 0.9800
O7—C1—C2 107.8 (2) C31—C30—C29 105.27 (17)
O7—C1—C11 108.43 (19) C31—C30—H30A 110.7
C2—C1—C11 117.1 (2) C29—C30—H30A 110.7
O7—C1—H1 107.7 C31—C30—H30B 110.7
C2—C1—H1 107.7 C29—C30—H30B 110.7
C11—C1—H1 107.7 H30A—C30—H30B 108.8
C3—C2—C1 113.8 (2) C30—C31—C32 111.15 (18)
C3—C2—H2A 108.8 C30—C31—C41 102.96 (16)
C1—C2—H2A 108.8 C32—C31—C41 110.98 (16)
C3—C2—H2B 108.8 C30—C31—H31 110.5
C1—C2—H2B 108.8 C32—C31—H31 110.5
H2A—C2—H2B 107.7 C41—C31—H31 110.5
C4—C3—C2 109.3 (2) O11—C32—C31 105.12 (17)
C4—C3—H3A 109.8 O11—C32—C39 107.97 (17)
C2—C3—H3A 109.8 C31—C32—C39 112.04 (19)
C4—C3—H3B 109.8 O11—C32—C33 108.49 (19)
C2—C3—H3B 109.8 C31—C32—C33 110.21 (17)
H3A—C3—H3B 108.3 C39—C32—C33 112.65 (18)
O2—C4—C3 109.8 (2) O14—C33—C38 111.30 (17)
O2—C4—C5 101.74 (18) O14—C33—C34 108.18 (17)
C3—C4—C5 110.8 (2) C38—C33—C34 102.86 (17)
O2—C4—C18 110.4 (2) O14—C33—C32 113.09 (19)
C3—C4—C18 114.4 (2) C38—C33—C32 109.54 (18)
C5—C4—C18 108.98 (19) C34—C33—C32 111.41 (17)
C4—C5—C6 108.03 (19) C33—C34—C36 103.19 (17)
C4—C5—C11 108.83 (18) C33—C34—C35 117.85 (16)
C6—C5—C11 105.32 (17) C36—C34—C35 116.19 (18)
C4—C5—H5 111.5 C33—C34—H34 106.2
C6—C5—H5 111.5 C36—C34—H34 106.2
C11—C5—H5 111.5 C35—C34—H34 106.2
C7—C6—C5 104.39 (17) C41—C35—C29 98.14 (16)
C7—C6—H6A 110.9 C41—C35—C25 116.01 (17)
C5—C6—H6A 110.9 C29—C35—C25 112.82 (16)
C7—C6—H6B 110.9 C41—C35—C34 110.27 (16)
C5—C6—H6B 110.9 C29—C35—C34 111.05 (16)
H6A—C6—H6B 108.9 C25—C35—C34 108.30 (16)
C8—C7—C6 110.69 (18) C37—C36—C34 106.70 (18)
C8—C7—C17 111.72 (18) C37—C36—H36A 110.4
C6—C7—C17 103.77 (17) C34—C36—H36A 110.4
C8—C7—H7 110.2 C37—C36—H36B 110.4
C6—C7—H7 110.2 C34—C36—H36B 110.4
C17—C7—H7 110.2 H36A—C36—H36B 108.6
O4—C8—C7 105.52 (18) C38—C37—C40 113.19 (19)
O4—C8—C15 108.17 (18) C38—C37—C36 99.25 (18)
C7—C8—C15 111.87 (19) C40—C37—C36 110.85 (18)
O4—C8—C9 108.27 (19) C38—C37—H37 111.0
C7—C8—C9 109.72 (18) C40—C37—H37 111.0
C15—C8—C9 112.9 (2) C36—C37—H37 111.0
O3—C9—C14 110.43 (18) O12—C38—C37 118.60 (19)
O3—C9—C10 108.94 (18) O12—C38—C33 109.01 (18)
C14—C9—C10 102.78 (19) C37—C38—C33 102.50 (17)
O3—C9—C8 112.8 (2) O12—C38—H38 108.8
C14—C9—C8 109.8 (2) C37—C38—H38 108.8
C10—C9—C8 111.68 (17) C33—C38—H38 108.8
C9—C10—C12 103.03 (19) C40—C39—C32 118.16 (18)
C9—C10—C11 117.51 (18) C40—C39—H39A 107.8
C12—C10—C11 115.81 (19) C32—C39—H39A 107.8
C9—C10—H10 106.6 C40—C39—H39B 107.8
C12—C10—H10 106.6 C32—C39—H39B 107.8
C11—C10—H10 106.6 H39A—C39—H39B 107.1
C17—C11—C1 116.23 (18) O13—C40—C39 110.64 (18)
C17—C11—C5 98.06 (18) O13—C40—C37 108.11 (18)
C1—C11—C5 112.57 (18) C39—C40—C37 113.07 (19)
C17—C11—C10 109.21 (17) O13—C40—H40 108.3
C1—C11—C10 108.58 (18) C39—C40—H40 108.3
C5—C11—C10 111.92 (18) C37—C40—H40 108.3
C13—C12—C10 106.9 (2) N4—C41—C35 108.80 (16)
C13—C12—H12A 110.3 N4—C41—C31 115.46 (16)
C10—C12—H12A 110.3 C35—C41—C31 100.84 (16)
C13—C12—H12B 110.3 N4—C41—H41 110.4
C10—C12—H12B 110.3 C35—C41—H41 110.4
H12A—C12—H12B 108.6 C31—C41—H41 110.4
C14—C13—C16 112.5 (2) N4—C42—C28 113.15 (17)
C14—C13—C12 99.8 (2) N4—C42—H42A 108.9
C16—C13—C12 111.2 (2) C28—C42—H42A 108.9
C14—C13—H13 111.0 N4—C42—H42B 108.9
C16—C13—H13 111.0 C28—C42—H42B 108.9
C12—C13—H13 111.0 H42A—C42—H42B 107.8
O5—C14—C9 108.6 (2) O8—C43—O9 122.2 (2)
O5—C14—C13 117.9 (2) O8—C43—C1'' 125.3 (2)
C9—C14—C13 102.86 (19) O9—C43—C1'' 112.53 (19)
O5—C14—H14 109.0 O10—C44—H44A 109.5
C9—C14—H14 109.0 O10—C44—H44B 109.5
C13—C14—H14 109.0 H44A—C44—H44B 109.5
C16—C15—C8 119.1 (2) O10—C44—H44C 109.5
C16—C15—H15A 107.5 H44A—C44—H44C 109.5
C8—C15—H15A 107.5 H44B—C44—H44C 109.5
C16—C15—H15B 107.5 O12—C45—H45A 109.5
C8—C15—H15B 107.5 O12—C45—H45B 109.5
H15A—C15—H15B 107.0 H45A—C45—H45B 109.5
O6—C16—C15 111.0 (2) O12—C45—H45C 109.5
O6—C16—C13 107.2 (2) H45A—C45—H45C 109.5
C15—C16—C13 113.5 (2) H45B—C45—H45C 109.5
O6—C16—H16 108.3 O13—C46—H46A 109.5
C15—C16—H16 108.3 O13—C46—H46B 109.5
C13—C16—H16 108.3 H46A—C46—H46B 109.5
N2—C17—C11 108.60 (17) O13—C46—H46C 109.5
N2—C17—C7 115.47 (18) H46A—C46—H46C 109.5
C11—C17—C7 100.71 (17) H46B—C46—H46C 109.5
N2—C17—H17 110.5 N4—C47—C48 114.3 (2)
C11—C17—H17 110.5 N4—C47—H47A 108.7
C7—C17—H17 110.5 C48—C47—H47A 108.7
N2—C18—C4 112.4 (2) N4—C47—H47B 108.7
N2—C18—H18A 109.1 C48—C47—H47B 108.7
C4—C18—H18A 109.1 H47A—C47—H47B 107.6
N2—C18—H18B 109.1 C47—C48—H48A 109.5
C4—C18—H18B 109.1 C47—C48—H48B 109.5
H18A—C18—H18B 107.8 H48A—C48—H48B 109.5
O1—C19—O2 123.0 (3) C47—C48—H48C 109.5
O1—C19—C1' 125.6 (3) H48A—C48—H48C 109.5
O2—C19—C1' 111.4 (2) H48B—C48—H48C 109.5
O7—C20—H20A 109.5 C6'—C1'—C2' 118.2 (3)
O7—C20—H20B 109.5 C6'—C1'—C19 119.7 (3)
H20A—C20—H20B 109.5 C2'—C1'—C19 122.0 (3)
O7—C20—H20C 109.5 N1—C2'—C3' 119.0 (3)
H20A—C20—H20C 109.5 N1—C2'—C1' 122.4 (3)
H20B—C20—H20C 109.5 C3'—C2'—C1' 118.6 (3)
O6—C21—H21A 109.5 C4'—C3'—C2' 121.3 (3)
O6—C21—H21B 109.5 C4'—C3'—H3' 119.3
H21A—C21—H21B 109.5 C2'—C3'—H3' 119.3
O6—C21—H21C 109.5 C3'—C4'—C5' 120.0 (4)
H21A—C21—H21C 109.5 C3'—C4'—H4' 120.0
H21B—C21—H21C 109.5 C5'—C4'—H4' 120.0
O5—C22—H22A 109.5 C6'—C5'—C4' 120.1 (4)
O5—C22—H22B 109.5 C6'—C5'—H5' 120.0
H22A—C22—H22B 109.5 C4'—C5'—H5' 120.0
O5—C22—H22C 109.5 C5'—C6'—C1' 121.7 (3)
H22A—C22—H22C 109.5 C5'—C6'—H6' 119.1
H22B—C22—H22C 109.5 C1'—C6'—H6' 119.1
N2—C23—C24 113.5 (2) C6''—C1''—C2'' 118.3 (2)
N2—C23—H23A 108.9 C6''—C1''—C43 120.7 (2)
C24—C23—H23A 108.9 C2''—C1''—C43 120.9 (2)
N2—C23—H23B 108.9 N3—C2''—C3'' 119.9 (3)
C24—C23—H23B 108.9 N3—C2''—C1'' 122.0 (3)
H23A—C23—H23B 107.7 C3''—C2''—C1'' 118.1 (3)
C23—C24—H24A 109.5 C4''—C3''—C2'' 121.7 (3)
C23—C24—H24B 109.5 C4''—C3''—H3'' 119.2
H24A—C24—H24B 109.5 C2''—C3''—H3'' 119.2
C23—C24—H24C 109.5 C3''—C4''—C5'' 120.1 (3)
H24A—C24—H24C 109.5 C3''—C4''—H4'' 120.0
H24B—C24—H24C 109.5 C5''—C4''—H4'' 120.0
O10—C25—C26 108.00 (17) C6''—C5''—C4'' 119.7 (3)
O10—C25—C35 109.78 (16) C6''—C5''—H5'' 120.1
C26—C25—C35 116.81 (17) C4''—C5''—H5'' 120.1
O10—C25—H25 107.3 C5''—C6''—C1'' 122.1 (2)
C26—C25—H25 107.3 C5''—C6''—H6'' 119.0
C35—C25—H25 107.3 C1''—C6''—H6'' 119.0
C27—C26—C25 113.19 (19) C2'—N1—H1A 108.9
C27—C26—H26A 108.9 C2'—N1—H1B 109.3
C25—C26—H26A 108.9 H1A—N1—H1B 109.5
C27—C26—H26B 108.9 C23—N2—C18 111.77 (19)
C25—C26—H26B 108.9 C23—N2—C17 114.02 (19)
H26A—C26—H26B 107.8 C18—N2—C17 116.80 (18)
C26—C27—C28 109.07 (18) C2''—N3—H3C 108.5
C26—C27—H27A 109.9 C2''—N3—H3D 109.0
C28—C27—H27A 109.9 H3C—N3—H3D 109.5
C26—C27—H27B 109.9 C47—N4—C42 109.67 (17)
C28—C27—H27B 109.9 C47—N4—C41 114.24 (17)
H27A—C27—H27B 108.3 C42—N4—C41 117.19 (17)
O9—C28—C27 109.62 (17) C19—O2—C4 124.4 (2)
O9—C28—C29 102.89 (16) C9—O3—H3 109.5
C27—C28—C29 110.14 (18) C8—O4—H4 109.5
O9—C28—C42 110.62 (17) C22—O5—C14 113.9 (2)
C27—C28—C42 114.03 (18) C21—O6—C16 112.6 (2)
C29—C28—C42 108.97 (17) C20—O7—C1 114.2 (2)
C28—C29—C30 108.75 (17) C43—O9—C28 122.13 (17)
C28—C29—C35 109.14 (17) C25—O10—C44 113.1 (2)
C30—C29—C35 104.76 (17) C32—O11—H11 109.4
C28—C29—H29 111.3 C45—O12—C38 112.77 (19)
C30—C29—H29 111.3 C46—O13—C40 112.65 (18)
C35—C29—H29 111.3 C33—O14—H14A 109.3
O7—C1—C2—C3 161.3 (2) O14—C33—C34—C35 −89.7 (2)
C11—C1—C2—C3 38.9 (3) C38—C33—C34—C35 152.49 (18)
C1—C2—C3—C4 −51.2 (3) C32—C33—C34—C35 35.2 (3)
C2—C3—C4—O2 177.0 (2) C28—C29—C35—C41 −74.90 (19)
C2—C3—C4—C5 65.4 (3) C30—C29—C35—C41 41.42 (19)
C2—C3—C4—C18 −58.2 (3) C28—C29—C35—C25 47.8 (2)
O2—C4—C5—C6 65.3 (2) C30—C29—C35—C25 164.15 (17)
C3—C4—C5—C6 −178.0 (2) C28—C29—C35—C34 169.64 (16)
C18—C4—C5—C6 −51.3 (2) C30—C29—C35—C34 −74.0 (2)
O2—C4—C5—C11 179.17 (18) O10—C25—C35—C41 −48.4 (2)
C3—C4—C5—C11 −64.2 (3) C26—C25—C35—C41 74.9 (2)
C18—C4—C5—C11 62.5 (2) O10—C25—C35—C29 −160.53 (17)
C4—C5—C6—C7 101.3 (2) C26—C25—C35—C29 −37.2 (3)
C11—C5—C6—C7 −14.9 (2) O10—C25—C35—C34 76.1 (2)
C5—C6—C7—C8 102.43 (19) C26—C25—C35—C34 −160.53 (19)
C5—C6—C7—C17 −17.6 (2) C33—C34—C35—C41 −49.7 (2)
C6—C7—C8—O4 64.9 (2) C36—C34—C35—C41 73.5 (2)
C17—C7—C8—O4 179.98 (18) C33—C34—C35—C29 58.0 (2)
C6—C7—C8—C15 −177.73 (19) C36—C34—C35—C29 −178.83 (17)
C17—C7—C8—C15 −62.6 (2) C33—C34—C35—C25 −177.63 (18)
C6—C7—C8—C9 −51.6 (2) C36—C34—C35—C25 −54.4 (2)
C17—C7—C8—C9 63.5 (2) C33—C34—C36—C37 7.3 (2)
O4—C8—C9—O3 −31.9 (2) C35—C34—C36—C37 −123.20 (19)
C7—C8—C9—O3 82.8 (2) C34—C36—C37—C38 −34.7 (2)
C15—C8—C9—O3 −151.70 (19) C34—C36—C37—C40 84.5 (2)
O4—C8—C9—C14 91.7 (2) C40—C37—C38—O12 52.1 (3)
C7—C8—C9—C14 −153.64 (19) C36—C37—C38—O12 169.60 (18)
C15—C8—C9—C14 −28.1 (3) C40—C37—C38—C33 −68.0 (2)
O4—C8—C9—C10 −155.01 (18) C36—C37—C38—C33 49.5 (2)
C7—C8—C9—C10 −40.3 (3) O14—C33—C38—O12 71.7 (2)
C15—C8—C9—C10 85.2 (2) C34—C33—C38—O12 −172.71 (17)
O3—C9—C10—C12 143.00 (19) C32—C33—C38—O12 −54.1 (2)
C14—C9—C10—C12 25.9 (2) O14—C33—C38—C37 −161.82 (18)
C8—C9—C10—C12 −91.8 (2) C34—C33—C38—C37 −46.2 (2)
O3—C9—C10—C11 −88.4 (2) C32—C33—C38—C37 72.4 (2)
C14—C9—C10—C11 154.5 (2) O11—C32—C39—C40 −143.67 (19)
C8—C9—C10—C11 36.9 (3) C31—C32—C39—C40 101.0 (2)
O7—C1—C11—C17 −47.8 (3) C33—C32—C39—C40 −23.9 (3)
C2—C1—C11—C17 74.3 (3) C32—C39—C40—O13 150.93 (19)
O7—C1—C11—C5 −159.75 (19) C32—C39—C40—C37 29.5 (3)
C2—C1—C11—C5 −37.6 (3) C38—C37—C40—O13 −105.1 (2)
O7—C1—C11—C10 75.8 (2) C36—C37—C40—O13 144.42 (19)
C2—C1—C11—C10 −162.1 (2) C38—C37—C40—C39 17.8 (3)
C4—C5—C11—C17 −74.4 (2) C36—C37—C40—C39 −92.7 (2)
C6—C5—C11—C17 41.2 (2) C29—C35—C41—N4 69.81 (19)
C4—C5—C11—C1 48.4 (2) C25—C35—C41—N4 −50.6 (2)
C6—C5—C11—C1 164.07 (18) C34—C35—C41—N4 −174.11 (16)
C4—C5—C11—C10 171.08 (18) C29—C35—C41—C31 −52.03 (17)
C6—C5—C11—C10 −73.3 (2) C25—C35—C41—C31 −172.41 (16)
C9—C10—C11—C17 −51.6 (3) C34—C35—C41—C31 64.05 (19)
C12—C10—C11—C17 70.7 (3) C30—C31—C41—N4 −73.1 (2)
C9—C10—C11—C1 −179.26 (19) C32—C31—C41—N4 167.96 (17)
C12—C10—C11—C1 −57.0 (3) C30—C31—C41—C35 43.99 (19)
C9—C10—C11—C5 55.9 (3) C32—C31—C41—C35 −75.0 (2)
C12—C10—C11—C5 178.2 (2) O9—C28—C42—N4 −153.09 (17)
C9—C10—C12—C13 3.5 (2) C27—C28—C42—N4 82.8 (2)
C11—C10—C12—C13 −126.2 (2) C29—C28—C42—N4 −40.7 (2)
C10—C12—C13—C14 −31.2 (3) O1—C19—C1'—C6' 179.2 (3)
C10—C12—C13—C16 87.7 (3) O2—C19—C1'—C6' −0.1 (4)
O3—C9—C14—O5 71.1 (2) O1—C19—C1'—C2' 3.2 (5)
C10—C9—C14—O5 −172.86 (18) O2—C19—C1'—C2' −176.2 (3)
C8—C9—C14—O5 −53.9 (3) C6'—C1'—C2'—N1 179.3 (3)
O3—C9—C14—C13 −163.2 (2) C19—C1'—C2'—N1 −4.6 (5)
C10—C9—C14—C13 −47.2 (2) C6'—C1'—C2'—C3' −1.6 (4)
C8—C9—C14—C13 71.8 (2) C19—C1'—C2'—C3' 174.5 (3)
C16—C13—C14—O5 49.6 (3) N1—C2'—C3'—C4' −179.0 (4)
C12—C13—C14—O5 167.5 (2) C1'—C2'—C3'—C4' 1.9 (5)
C16—C13—C14—C9 −69.9 (3) C2'—C3'—C4'—C5' −0.3 (7)
C12—C13—C14—C9 48.1 (2) C3'—C4'—C5'—C6' −1.4 (8)
O4—C8—C15—C16 −140.2 (2) C4'—C5'—C6'—C1' 1.6 (8)
C7—C8—C15—C16 104.0 (2) C2'—C1'—C6'—C5' −0.1 (6)
C9—C8—C15—C16 −20.4 (3) C19—C1'—C6'—C5' −176.3 (4)
C8—C15—C16—O6 144.3 (2) O8—C43—C1''—C6'' 174.7 (2)
C8—C15—C16—C13 23.5 (3) O9—C43—C1''—C6'' −4.4 (3)
C14—C13—C16—O6 −100.5 (3) O8—C43—C1''—C2'' −3.5 (4)
C12—C13—C16—O6 148.5 (2) O9—C43—C1''—C2'' 177.4 (2)
C14—C13—C16—C15 22.4 (3) C6''—C1''—C2''—N3 178.6 (3)
C12—C13—C16—C15 −88.6 (3) C43—C1''—C2''—N3 −3.1 (4)
C1—C11—C17—N2 −50.0 (3) C6''—C1''—C2''—C3'' 0.6 (4)
C5—C11—C17—N2 70.1 (2) C43—C1''—C2''—C3'' 178.9 (3)
C10—C11—C17—N2 −173.27 (17) N3—C2''—C3''—C4'' −179.6 (3)
C1—C11—C17—C7 −171.74 (19) C1''—C2''—C3''—C4'' −1.6 (5)
C5—C11—C17—C7 −51.62 (19) C2''—C3''—C4''—C5'' 1.8 (5)
C10—C11—C17—C7 65.0 (2) C3''—C4''—C5''—C6'' −1.1 (5)
C8—C7—C17—N2 167.96 (18) C4''—C5''—C6''—C1'' 0.2 (4)
C6—C7—C17—N2 −72.8 (2) C2''—C1''—C6''—C5'' 0.0 (4)
C8—C7—C17—C11 −75.3 (2) C43—C1''—C6''—C5'' −178.3 (2)
C6—C7—C17—C11 44.0 (2) C24—C23—N2—C18 157.0 (2)
O2—C4—C18—N2 −153.59 (18) C24—C23—N2—C17 −67.8 (3)
C3—C4—C18—N2 82.0 (3) C4—C18—N2—C23 176.49 (19)
C5—C4—C18—N2 −42.6 (3) C4—C18—N2—C17 42.6 (3)
O10—C25—C26—C27 164.22 (19) C11—C17—N2—C23 168.01 (19)
C35—C25—C26—C27 40.0 (3) C7—C17—N2—C23 −79.8 (3)
C25—C26—C27—C28 −53.2 (3) C11—C17—N2—C18 −59.1 (2)
C26—C27—C28—O9 179.43 (18) C7—C17—N2—C18 53.0 (3)
C26—C27—C28—C29 66.9 (2) C48—C47—N4—C42 165.8 (2)
C26—C27—C28—C42 −55.9 (3) C48—C47—N4—C41 −60.4 (3)
O9—C28—C29—C30 65.5 (2) C28—C42—N4—C47 172.51 (19)
C27—C28—C29—C30 −177.69 (18) C28—C42—N4—C41 40.2 (2)
C42—C28—C29—C30 −51.9 (2) C35—C41—N4—C47 172.30 (19)
O9—C28—C29—C35 179.26 (16) C31—C41—N4—C47 −75.2 (2)
C27—C28—C29—C35 −63.9 (2) C35—C41—N4—C42 −57.4 (2)
C42—C28—C29—C35 61.8 (2) C31—C41—N4—C42 55.0 (2)
C28—C29—C30—C31 101.63 (19) O1—C19—O2—C4 −7.9 (4)
C35—C29—C30—C31 −15.0 (2) C1'—C19—O2—C4 171.5 (2)
C29—C30—C31—C32 101.46 (19) C3—C4—O2—C19 73.0 (3)
C29—C30—C31—C41 −17.4 (2) C5—C4—O2—C19 −169.6 (2)
C30—C31—C32—O11 67.1 (2) C18—C4—O2—C19 −54.0 (3)
C41—C31—C32—O11 −179.00 (17) C9—C14—O5—C22 −160.9 (3)
C30—C31—C32—C39 −175.93 (17) C13—C14—O5—C22 82.7 (3)
C41—C31—C32—C39 −62.0 (2) C15—C16—O6—C21 68.2 (4)
C30—C31—C32—C33 −49.7 (2) C13—C16—O6—C21 −167.3 (3)
C41—C31—C32—C33 64.3 (2) C2—C1—O7—C20 81.8 (3)
O11—C32—C33—O14 −33.1 (2) C11—C1—O7—C20 −150.6 (3)
C31—C32—C33—O14 81.5 (2) O8—C43—O9—C28 3.2 (3)
C39—C32—C33—O14 −152.54 (18) C1''—C43—O9—C28 −177.64 (18)
O11—C32—C33—C38 91.7 (2) C27—C28—O9—C43 70.0 (2)
C31—C32—C33—C38 −153.70 (18) C29—C28—O9—C43 −172.83 (18)
C39—C32—C33—C38 −27.8 (2) C42—C28—O9—C43 −56.6 (2)
O11—C32—C33—C34 −155.17 (17) C26—C25—O10—C44 79.8 (2)
C31—C32—C33—C34 −40.6 (2) C35—C25—O10—C44 −151.8 (2)
C39—C32—C33—C34 85.4 (2) C37—C38—O12—C45 64.2 (3)
O14—C33—C34—C36 140.79 (18) C33—C38—O12—C45 −179.2 (2)
C38—C33—C34—C36 22.9 (2) C39—C40—O13—C46 75.9 (3)
C32—C33—C34—C36 −94.3 (2) C37—C40—O13—C46 −159.8 (2)