| Bruker SMART CCD area-detector diffractometer | 2119 independent reflections |
| Radiation source: fine-focus sealed tube | 2027 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.017 |
| Detector resolution: 10.0 pixels mm-1 | θmax = 25.0°, θmin = 1.8° |
| ω and φ scans | h = −5→5 |
| Absorption correction: ψ scan (SADABS; Sheldrick, 2007) | k = −13→13 |
| Tmin = 0.770, Tmax = 1.000 | l = −13→16 |
| 4426 measured reflections |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.