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. 2015 Jul 31;71(Pt 8):o617–o618. doi: 10.1107/S2056989015014103
Bruker Kappa APEXII CCD diffractometer 2001 independent reflections
Radiation source: fine-focus sealed tube 1356 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.051
ω and φ scan θmax = 25.0°, θmin = 2.2°
Absorption correction: multi-scan (SADABS; Bruker, 2004) h = −15→14
Tmin = 0.961, Tmax = 0.979 k = −10→10
27493 measured reflections l = −22→22