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. 2015 Jul 31;71(Pt 8):o617–o618. doi: 10.1107/S2056989015014103
Refinement on F2 Hydrogen site location: inferred from neighbouring sites
Least-squares matrix: full H-atom parameters constrained
R[F2 > 2σ(F2)] = 0.044 w = 1/[σ2(Fo2) + (0.0513P)2 + 1.4242P] where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.138 (Δ/σ)max < 0.001
S = 1.15 Δρmax = 0.19 e Å3
2001 reflections Δρmin = −0.21 e Å3
173 parameters Extinction correction: SHELXL2014 (Sheldrick, 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
0 restraints Extinction coefficient: 0.0072 (15)