Table 5.
Data Statistics for the Crystal of the Complexes of Dpo4 and 13/18-mer-dG1,8 in the Presence or Absence of dCTP
| space group | P31 |
|---|---|
| cell dimens | |
| a, b, c (Å) | 56.39, 56.39, 288.77 |
| α, β, γ (deg) | 90.00, 90.00, 120.00 |
| refinement | |
| resolution (Å)a | 50.00–2.20 (2.28–2.20) |
| Rmergeb | 14.30 (83.90) |
| I/σ (I) | 11.34 (3.11) |
| completeness (%) | 99.8 (100.00) |
| redundancy | 5.80 (6.80) |
| resolution (Å) | 20.23–2.20 (2.25–2.20) |
| no. of reflns | 49 297 (2649) |
| Rwork/Rfreec | 0.2015/0.2500 |
| no. of atoms | |
| protein | 5516 |
| DNA-dG1,8 | 1225 |
| dCTP | 28 |
| B factors | |
| protein | 43.21 |
| DNA-dG1,8 | 48.96 |
| dCTP | 30.2 |
| rms deviations | |
| bond lengths (Å) | 0.008 |
| bond angles (def) | 1.294 |
a
Highest resolution shell is shown in parentheses.
b
Rmerge = Σ|I – 〈I〉|/ΣI, where I is the integrated intensity of each reflection.
c
R value = Σ║Fo | – |Fc║/Σ|Fo|, where Fo and Fc are observed and calculated structure factor amplitudes, respectively.