Table 2.
13C NMR (150 MHz, DMSO-d6) Data for Compounds 1–5.
Carbon | 1 | 2 | 3 | 4 | 5 |
---|---|---|---|---|---|
1 | 95.8, CH | 123.5, qC | 209.6, qC | 208.7, qC | 208.7, qC |
2 | 79.2, CH | 130.3, CH | 129.4, CH | 128.4, CH | 135.1, CH |
3 | 77.5, CH | 115.3, CH | 180.3, qC | 181.6, qC | 169.3, qC |
4 | 150.7, qC | 157.4, qC | 31.6, CH2 | 31.0, CH2 | 26.6, CH2 |
5 | 109.4, CH | 115.3, CH | 35.2, CH2 | 34.9, CH2 | 34.7, CH2 |
6 | 107.3, CH | 130.3, CH | 28.4, CH2 | 28.0, CH2 | 137.9, CH |
7 | 155.9, qC | 137.7, qC | 31.5, CH2 | 30.9, CH2 | 126.4, CH |
8 | 55.6, CH2 | 136.0, CH | 172.0, qC | 171.9, qC | 166.7, qC |
9 | 16.4, CH3 | 149.6, qC | 65.2, CH2 | 64.9, CH2 | |
10 | 16.5, CH3 | 117.0, CH | 35.0, CH2 | 33.5, CH2 | |
11 | 110.1, CH | 137.5, qC | 127.8, qC | ||
12 | 159.0, qC | 128.8, CH | 129.7, CH | ||
13 | 55.8, CH2 | 128.5, CH | 115.1, CH | ||
14 | 193.4, CH | 126.7, CH | 155.9, qC | ||
15 | 128.5, CH | 115.1, CH | |||
16 | 128.8, CH | 129.7, CH |