Table 3.
Entry | Phosphorylating agent | Concentration of Mg2+, M | Yield, %* |
1 | ATP.2Na | No MgCl2 | 36 ± 1 |
2 | ATP.2Na | 0.25 | 23 ± 1 |
3 | ATP.2Na | 1.0 | 32 ± 1 |
4 | ATP.2Na | 2.0 | 50 ± 0.5 |
ATP (0.025 M), MgCl2, H2O:MeOH (1:1), 60 °C, 48 h.
NMR yield.
Entry | Phosphorylating agent | Concentration of Mg2+, M | Yield, %* |
1 | ATP.2Na | No MgCl2 | 36 ± 1 |
2 | ATP.2Na | 0.25 | 23 ± 1 |
3 | ATP.2Na | 1.0 | 32 ± 1 |
4 | ATP.2Na | 2.0 | 50 ± 0.5 |
ATP (0.025 M), MgCl2, H2O:MeOH (1:1), 60 °C, 48 h.
NMR yield.