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. 2015 Sep 23;71(Pt 10):1235–1241. doi: 10.1107/S2053230X1501537X

Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source Beamline I911-3, MAX-lab
Wavelength () 0.9199
Temperature (K) 110
Detector CCD
Crystal-to-detector distance (mm) 217.88
Rotation range per image () 0.5
Total rotation range () 100
Space group P4322
a, b, c () 91.52, 91.52, 184.59
, , () 90, 90, 90
Mosaicity () 0.240
Z 6
Resolution range () 41.211.85 (1.901.85)
Total No. of reflections 510190 (5674)
No. of unique reflections 67728 (896)
Completeness (%) 100.0 (99.8)
Multiplicity 7.5 (5.6)
I/(I) 12.200 (2.6)
R r.i.m. 0.118 (0.6179)
R p.i.m. 0.043 (0.306)
Overall B factor from Wilson plot (2) 20.150