Table 3. Data collection and processing.
Values in parentheses are for the outer shell.
| Diffraction source | ID30A-3, ESRF |
| Wavelength () | 0.9677 |
| Temperature (K) | 100 |
| Detector | Pilatus3 2M |
| Crystal-to-detector distance (mm) | 148.66 |
| Rotation range per image () | 0.1 |
| Total rotation range () | 130 |
| Exposure time per image (s) | 0.02 |
| Space group | P21212 or P212121 |
| a, b, c () | 56.3, 60.4, 56.8 |
| , , () | 90, 90, 90 |
| Mosaicity () | 0.047 |
| Resolution range () | 100.01.4 (1.451.40) |
| Total No. of reflections | 183274 (18114) |
| No. of unique reflections | 38706 (3801) |
| Completeness (%) | 99.3 (98.6) |
| Multiplicity | 4.7 (4.8) |
| I/(I) | 13.2 (1.7) |
| R meas † (%) | 6.3 (91.6) |
| Overall B factor from Wilson plot (2) | 24.6 |
| Matthews coefficient V M (3Da1) | 1.75 |
| Solvent content (%) | 29.6 |
†
R
meas = 
.