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. 2015 Sep 23;71(Pt 10):1335–1340. doi: 10.1107/S2053230X15016799

Table 2. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source Spring-8, Japan
Wavelength () 0.8
Temperature (K) 100
Detector MAR Mosaic 225 CCD
Crystal-to-detector distance (mm) 100
Rotation range per image () 0.5
Total rotation range () 180
Exposure time per image (s) 0.5
Space group P41212
a, b, c () 79.380, 79.380, 100.370
, , () 90.00, 90.00, 90.00
Mosaicity () 0.09
Resolution range () 301.25 (1.321.25)
Total No. of reflections 1195243
No. of unique reflections 88471
Completeness (%) 99.4 (96.4)
Multiplicity 13.51 (7.44)
I/(I) 16.1 (3.2)
R r.i.m. 0.111 (0.498)
Overall B factor from Wilson plot (2) 8.3