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. Author manuscript; available in PMC: 2015 Oct 13.
Published in final edited form as: Inorg Chem. 2015 May 22;54(19):9256–9262. doi: 10.1021/acs.inorgchem.5b00645

Figure 4.

Figure 4

(left) Cyclic voltammagram of (CP3)Co(N2) (5) scanning oxidatively at 100 mV/sec in THF with 0.1 M TBAPF6 electrolyte. (middle) UV-vis spectra of 6 under 1 atm N2 (solid line) and under static vacuum (dotted line: after three freeze-pump-thaw cycles). Spectra were collected on a 1 mM solution of 6 in THF at 298 K. (right) X-band EPR spectrum of 6 collected under 1 atm N2 in 2-Me-THF at 80 K. No low-field features were detected.