Table 1.
Compounds | R | R′ | M.p. (°C) | Overall yield (%) |
---|---|---|---|---|
5a | Phenyl | H | 224–226 | 80 |
5b | Phenyl | Cl | 254–258 | 84 |
5c | Phenyl | OH | 246–248 | 76 |
5d | Phenyl | NO2 | 241–245 | 79 |
5e | Phenyl | OCH3 | 252–253 | 68 |
5f | Phenyl-4-NO2 | H | 254–255 | 79 |
5g | Phenyl-4-NO2 | Cl | 257–259 | 76 |
5h | Phenyl-4-NO2 | OH | 259–260 | 86 |
5i | Phenyl-4-NO2 | NO2 | 258–260 | 84 |
5j | Phenyl-4-NO2 | OCH3 | 248–250 | 75 |
5k | Pyridin-2yl | H | 236–237 | 74 |
5l | Pyridin-2yl | Cl | 238–240 | 82 |
5m | Pyridin-2yl | OH | 258–259 | 72 |
5n | Pyridin-2yl | NO2 | 264–267 | 69 |
5o | Pyridin-2yl | OCH3 | 257–259 | 78 |