Table 1. Analysis conditions of gas chromatography-mass spectroscopy for the eight polycyclic aromatic hydrocarbons.
Instrument | Agilent Technologies 689ON/5975 MSD |
---|---|
| |
Column | HP-5MS 30 m 0.25 mm ID 0.25 μm |
Column oven temperature | 80 (1 min) → 245 (6/min) → 270 (30/min, hold 10 min) → 310 (10 min, post run) |
Carrier gas | Helium (1.0 mL/min) |
Injection volume and temperature | 1.0 μL (Splitless), 270 |
MS source temperature/MS quadrupole temperature | 230/150 |
MS mode | SIM |