Table 1.
Property | Isolated metabolite 1 | Authentic 6-aminopendimethalin | Isolated metabolite 2 | Authentic 3,4-dimethyl 2,6-dinitroaniline |
---|---|---|---|---|
TLC: R f values in different solvent systems | ||||
A: Hexane–ethyl acetate (1:1, v/v) | 0.87 | 0.87 | 0.73 | 0.74 |
B: Toluene-dioxan-acetic acid (90:20:4, v/v) | 0.93 | 0.94 | 0.83 | 0.83 |
UV absorption λ max (nm) | 229.43 | 229.43 | 234.42 | 234.42 |
HPLC retention time (min) | 7.63 | 7.63 | 1.39 | 1.40 |
MS M+ at m/z | 236, 220, 191 | 236, 220, 191 | 181, 121, 55 | 181, 121, 55 |