Table 1. NMR spectroscopic data of ergosterol (ARHPLC-1) in CDCL3.
Position | ARHPLC-1 (in CDCL3) | |
---|---|---|
1H (400Hz) | 13C (100Hz) | |
1 | 38.3 | |
2 | 32.0 | |
3 | 3.63 (m,1H) | 70.4 |
4 | 40.8 | |
5 | 139.7 | |
6 | 5.57 (d, J = 6.2Hz, 1H) | 119.5 |
7 | 5.38 (t, J = 8.5Hz, 1H) | 116.3 |
8 | 141.3 | |
9 | 46.2 | |
10 | 37.0 | |
11 | 21.1 | |
12 | 39.1 | |
13 | 42.8 | |
14 | 54.5 | |
15 | 23.0 | |
16 | 28.2 | |
17 | 55.7 | |
18 | 0.63 (s, 3H) | 12.0 |
19 | 0.94 (s, 3H) | 16.2 |
20 | 40.3 | |
21 | 1.03 (d, J = 6.5Hz, 3H) | 19.6 |
22 | 5.16 (m, 1H) | 132.0 |
23 | 5.24 (m, 1H) | 135.5 |
24 | 42.8 | |
25 | 33.1 | |
26 | 0.83 (s, 3H) | 21.1 |
27 | 0.82 (d, 3H) | 19.9 |
28 | 0.91(d, J = 6.9Hz, 3H) | 17.5 |