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. Author manuscript; available in PMC: 2016 Sep 1.
Published in final edited form as: Angew Chem Int Ed Engl. 2015 Sep 1;54(36):10555–10558. doi: 10.1002/anie.201504775

Table 1.

Electrochemical Oxidation of Amidesa

entry substrate product yield, % (ratiob)
1 graphic file with name nihms732629t1.jpg
3a
graphic file with name nihms732629t2.jpg
3b
93 (1:1)
2 graphic file with name nihms732629t3.jpg
4a
graphic file with name nihms732629t4.jpg
4b
57
3 graphic file with name nihms732629t5.jpg
5a
graphic file with name nihms732629t6.jpg
5b
91 (4:1)
4 graphic file with name nihms732629t7.jpg
6a
graphic file with name nihms732629t8.jpg
6b
63 (single isomer)
5 graphic file with name nihms732629t9.jpg
7a
graphic file with name nihms732629t10.jpg
7b
56 (1.7:1)
6 graphic file with name nihms732629t11.jpg
8a
graphic file with name nihms732629t12.jpg
8b
28 (1.5:1)
7 graphic file with name nihms732629t13.jpg
9a
graphic file with name nihms732629t14.jpg
9b
47 (single isomer)
8 graphic file with name nihms732629t15.jpg
10a
graphic file with name nihms732629t16.jpg
10b
40 (single isomer)
9 graphic file with name nihms732629t17.jpg
1a
graphic file with name nihms732629t18.jpg
1b
78 (single isomer)
10 graphic file with name nihms732629t19.jpg
11a
graphic file with name nihms732629t20.jpg
11b
65 (2.8:1)
11 graphic file with name nihms732629t21.jpg
12a
graphic file with name nihms732629t22.jpg
12b
19 (single isomer)
a

Conditions: MeOH, undivided cell, C anode/cathode, Et4NOTs or LiClO4.

b

Ratios approximated by 1H NMR; except where shown, diastereomeric structures were not determined.