Table 2. Examples of unit-cell parameters obtained from data processing with HKL-2000, XDS and MOSFLM in the proper symmetry, as well as symmetry reduced to P1.
For each data set the structure name, data resolution, total rotation range and detector type is given on the first line, followed by the unit-cell parameters refined in P1 and in higher symmetry by the three data-processing programs. Maximum deviations of the unit-cell lengths (a) (absolute and relative) and angles () between data processing in the two symmetries are given in the last three columns.
| Program | Space group | a () | b () | c () | () | () | () | (a) () | (a)/a (%) | () () |
|---|---|---|---|---|---|---|---|---|---|---|
| MFT, 1.70, 360, MAR300HS | ||||||||||
| HKL-2000 | P41212 | 61.553 | 61.553 | 106.990 | 90 | 90 | 90 | |||
| HKL-2000 | P1 | 61.577 | 61.565 | 106.990 | 90.007 | 89.991 | 89.932 | 0.024 | 0.04 | 0.068 |
| XDS | P41212 | 61.541 | 61.541 | 106.983 | 90 | 90 | 90 | |||
| XDS | P1 | 61.514 | 61.525 | 106.947 | 90.005 | 90.017 | 90.065 | 0.036 | 0.06 | 0.065 |
| MOSFLM | P41212 | 61.51 | 61.51 | 106.99 | 90 | 90 | 90 | |||
| MOSFLM | P1 | 61.44 | 61.58 | 106.97 | 90.02 | 89.93 | 90.00 | 0.07 | 0.11 | 0.07 |
| HPP_INO, 1.50, 200, MAR300HS | ||||||||||
| HKL-2000 | P21 | 61.933 | 89.337 | 92.326 | 90 | 96.985 | 90 | |||
| HKL-2000 | P1 | 61.905 | 89.318 | 92.326 | 89.924 | 97.008 | 90.101 | 0.028 | 0.04 | 0.101 |
| XDS | P21 | 61.931 | 89.364 | 92.365 | 90 | 97.005 | 90 | |||
| XDS | P1 | 61.908 | 89.331 | 92.334 | 90.090 | 97.002 | 89.920 | 0.033 | 0.04 | 0.090 |
| MOSFLM | P21 | 61.85 | 89.11 | 92.20 | 90 | 97.00 | 90 | |||
| MOSFLM | P1 | 61.86 | 89.13 | 92.22 | 89.94 | 97.00 | 90.06 | 0.02 | 0.02 | 0.06 |
| HPP_Ca_INO, 1.40, 250, MAR300HS | ||||||||||
| HKL-2000 | P21 | 61.972 | 89.450 | 92.224 | 90 | 96.857 | 90 | |||
| HKL-2000 | P1 | 61.968 | 89.430 | 92.208 | 90.156 | 96.863 | 90.041 | 0.020 | 0.02 | 0.156 |
| XDS | P21 | 62.024 | 89.458 | 92.230 | 90 | 96.914 | 90 | |||
| XDS | P1 | 62.027 | 89.467 | 92.228 | 90.118 | 96.909 | 90.009 | 0.009 | 0.01 | 0.118 |
| MOSFLM | P21 | 61.98 | 89.43 | 92.28 | 90 | 96.86 | 90 | |||
| MOSFLM | P1 | 61.95 | 89.38 | 92.12 | 89.83 | 96.85 | 89.98 | 0.16 | 0.02 | 0.17 |
| HPP_Mg_HOL, 1.44, 360, MAR300HS | ||||||||||
| HKL-2000 | P21 | 61.951 | 89.461 | 92.203 | 90 | 96.928 | 90 | |||
| HKL-2000 | P1 | 61.950 | 89.441 | 92.213 | 90.062 | 96.904 | 89.905 | 0.020 | 0.02 | 0.095 |
| XDS | P21 | 62.083 | 89.513 | 92.153 | 90 | 96.752 | 90 | |||
| XDS | P1 | 62.092 | 89.528 | 92.163 | 90.025 | 96.750 | 90.009 | 0.015 | 0.02 | 0.025 |
| MOSFLM | P21 | 61.94 | 89.26 | 92.08 | 90 | 96.90 | 90 | |||
| MOSFLM | P1 | 61.94 | 89.44 | 92.21 | 90.11 | 96.93 | 89.85 | 0.18 | 0.02 | 0.15 |
| HPP_Mg_HOLP, 1.44, 250, MAR300HS | ||||||||||
| HKL-2000 | P21 | 61.883 | 88.858 | 92.175 | 90 | 96.910 | 90 | |||
| HKL-2000 | P1 | 61.876 | 88.841 | 92.169 | 90.048 | 96.916 | 90.992 | 0.017 | 0.02 | 0.048 |
| XDS | P21 | 61.864 | 88.796 | 92.140 | 90 | 96.918 | 90 | |||
| XDS | P1 | 61.859 | 88.784 | 92.128 | 90.045 | 96.917 | 90.004 | 0.012 | 0.01 | 0.045 |
| MOSFLM | P21 | 61.88 | 88.83 | 92.20 | 90 | 96.87 | 90 | |||
| MOSFLM | P1 | 61.88 | 88.82 | 92.18 | 89.99 | 96.88 | 90.00 | 0.02 | 0.02 | 0.01 |
| HPP_Mg_INO, 1.50, 250, MAR300HS | ||||||||||
| HKL-2000 | P21 | 62.158 | 89.459 | 92.361 | 90 | 96.900 | 90 | |||
| HKL-2000 | P1 | 62.145 | 89.427 | 92.302 | 89.989 | 96.891 | 90.104 | 0.059 | 0.06 | 0.104 |
| XDS | P21 | 62.090 | 89.519 | 92.161 | 90 | 96.752 | 90 | |||
| XDS | P1 | 62.099 | 89.535 | 92.171 | 90.024 | 96.750 | 90.010 | 0.016 | 0.02 | 0.024 |
| MOSFLM | P21 | 62.02 | 89.16 | 92.13 | 90 | 96.90 | 90 | |||
| MOSFLM | P1 | 62.05 | 89.21 | 92.17 | 90.02 | 96.91 | 90.05 | 0.05 | 0.06 | 0.05 |
| HPP_Mg_soakHOLP, 1.43, 250, MAR300HS | ||||||||||
| HKL-2000 | P21 | 61.890 | 89.826 | 92.602 | 90 | 97.071 | 90 | |||
| HKL-2000 | P1 | 61.881 | 89.813 | 92.590 | 89.982 | 97.069 | 89.997 | 0.013 | 0.01 | 0.018 |
| XDS | P21 | 61.865 | 89.805 | 92.569 | 90 | 97.057 | 90 | |||
| XDS | P1 | 61.841 | 89.769 | 92.532 | 90.033 | 97.056 | 90.003 | 0.037 | 0.04 | 0.033 |
| MOSFLM | P21 | 61.91 | 89.90 | 92.64 | 90 | 97.07 | 90 | |||
| MOSFLM | P1 | 61.94 | 89.94 | 92.66 | 90.03 | 97.07 | 89.97 | 0.04 | 0.04 | 0.03 |
| HPP_Mg_paratone, 1.50, 360, MAR300HS | ||||||||||
| HKL-2000 | P4212 | 86.947 | 86.947 | 61.836 | 90 | 90 | 90 | |||
| HKL-2000 | P1 | 86.903 | 86.872 | 61.790 | 90.023 | 90.120 | 90.095 | 0.075 | 0.09 | 0.095 |
| XDS | P4212 | 86.993 | 86.993 | 61.862 | 90 | 90 | 90 | |||
| XDS | P1 | 86.821 | 86.868 | 61.765 | 90.123 | 90.018 | 90.085 | 0.172 | 0.20 | 0.123 |
| MOSFLM | P4212 | 87.00 | 87.00 | 61.82 | 90 | 90 | 90 | |||
| MOSFLM | P1 | 86.91 | 86.92 | 61.78 | 89.87 | 89.94 | 90.02 | 0.09 | 0.10 | 0.13 |
| PROTK, 1.30, 330, MAR300 | ||||||||||
| HKL-2000 | P43212 | 67.547 | 67.547 | 106.883 | 90 | 90 | 90 | |||
| HKL-2000 | P1 | 67.541 | 67.554 | 106.884 | 90.006 | 89.998 | 89.993 | 0.007 | 0.01 | 0.007 |
| XDS | P43212 | 67.550 | 67.550 | 106.886 | 90 | 90 | 90 | |||
| XDS | P1 | 67.543 | 67.557 | 106.886 | 90.003 | 90.006 | 90.005 | 0.007 | 0.01 | 0.006 |
| MOSFLM | P43212 | 67.54 | 67.54 | 106.87 | 90 | 90 | 90 | |||
| MOSFLM | P1 | 67.55 | 67.53 | 106.88 | 90.01 | 90.00 | 90.01 | 0.01 | 0.02 | 0.01 |
| LSS, 1.40, 200, MAR225 | ||||||||||
| HKL-2000 | P21 | 37.436 | 107.366 | 56.602 | 90 | 102.147 | 90 | |||
| HKL-2000 | P1 | 37.437 | 107.368 | 56.604 | 90.003 | 102.147 | 89.990 | 0.002 | 0.01 | 0.010 |
| XDS | P21 | 37.433 | 107.341 | 56.602 | 90 | 102.155 | 90 | |||
| XDS | P1 | 37.435 | 107.346 | 56.604 | 90.006 | 102.155 | 90.008 | 0.005 | 0.01 | 0.008 |
| MOSFLM | P21 | 37.42 | 107.31 | 56.61 | 90 | 102.15 | 90 | |||
| MOSFLM | P1 | 37.41 | 107.29 | 56.59 | 89.97 | 102.14 | 89.97 | 0.02 | 0.04 | 0.03 |
| RFP, 1.46, 200, MAR225 | ||||||||||
| HKL-2000 | P212121 | 52.336 | 53.156 | 106.466 | 90 | 90 | 90 | |||
| HKL-2000 | P1 | 52.337 | 53.155 | 106.466 | 90.006 | 89.997 | 89.985 | 0.001 | 0.01 | 0.015 |
| XDS | P212121 | 52.485 | 53.200 | 106.533 | 90 | 90 | 90 | |||
| XDS | P1 | 52.480 | 53.125 | 106.498 | 90.038 | 90.030 | 90.155 | 0.075 | 0.01 | 0.155 |
| MOSFLM | P212121 | 52.35 | 53.20 | 106.48 | 90 | 90 | 90 | |||
| MOSFLM | P1 | 52.36 | 53.20 | 106.47 | 89.99 | 90.02 | 89.98 | 0.01 | 0.02 | 0.02 |