Table 3.
Phase residuals in resolution shells. Images were taken on a K2 Summit DDD camera mounted on an F20 electron microscope in super-resolution mode at a magnification of 15,858x without binning using dose rates of 4, 8 and 20 counts/pixel/s. The phase residuals are given for merging combinations of seven images each of the indicated imaging conditions. For each resolution shell the phase residual (in degree, top number) and number of spots (bottom number) are given. The red lines indicate the resolution cut-off (~80º phase residual).
| 4+8 counts/pixel/s | 4+20 counts/pixel/s | 8+20 counts/pixel/s | 4+8+20 counts/pixel/s | |||||||
|---|---|---|---|---|---|---|---|---|---|---|
| # | DMIN | DMAX | all IQs | IQ-wght | all IQs | IQ-wght | all IQs | IQ-wght | all IQs | IQ-wght |
| 1 | 1000.0 | 13.4 | 30.7 | 26.9 | 16.7 | 14.3 | 31.4 | 26.4 | 31.4 | 27.8 |
| 1 | 471 | 471 | 470 | 470 | 473 | 473 | 707 | 707 | ||
| 2 | 13.4 | 9.5 | 29.4 | 27.4 | 28.9 | 24.8 | 30.7 | 27.0 | 32.0 | 28.6 |
| 2 | 524 | 524 | 518 | 518 | 524 | 524 | 783 | 783 | ||
| 3 | 9.5 | 7.7 | 31.3 | 29.4 | 24.7 | 23.4 | 28.9 | 26.8 | 29.4 | 27.6 |
| 3 | 525 | 525 | 524 | 524 | 523 | 523 | 786 | 786 | ||
| 4 | 7.7 | 6.7 | 25.7 | 22.4 | 23.4 | 18.6 | 24.1 | 20.6 | 24.8 | 21.1 |
| 4 | 495 | 495 | 488 | 488 | 493 | 493 | 738 | 738 | ||
| 5 | 6.7 | 6.0 | 41.2 | 38.3 | 34.3 | 28.3 | 38.2 | 35.0 | 39.4 | 36.0 |
| 5 | 511 | 511 | 508 | 508 | 513 | 513 | 766 | 766 | ||
| 6 | 6.0 | 5.5 | 29.7 | 25.5 | 28.9 | 21.9 | 27.6 | 21.4 | 29.1 | 23.7 |
| 6 | 421 | 421 | 410 | 410 | 413 | 413 | 622 | 622 | ||
| 7 | 5.5 | 5.1 | 35.1 | 28.4 | 32.4 | 23.6 | 33.2 | 25.9 | 34.3 | 27.1 |
| 7 | 526 | 526 | 518 | 518 | 514 | 514 | 779 | 779 | ||
| 8 | 5.1 | 4.7 | 40.9 | 32.8 | 39.9 | 29.9 | 39.8 | 31.5 | 40.8 | 32.4 |
| 8 | 466 | 466 | 437 | 437 | 455 | 455 | 679 | 679 | ||
| 9 | 4.7 | 4.5 | 47.5 | 43.3 | 41.8 | 37.1 | 44.6 | 37.2 | 46.9 | 41.6 |
| 9 | 496 | 496 | 470 | 470 | 492 | 492 | 729 | 729 | ||
| 10 | 4.5 | 4.2 | 48.3 | 37.1 | 52.4 | 38.5 | 48.2 | 35.0 | 51.2 | 38.1 |
| 10 | 434 | 434 | 414 | 414 | 436 | 436 | 642 | 642 | ||
| 11 | 4.2 | 4.0 | 61.5 | 48.1 | 58.2 | 46.2 | 59.4 | 42.5 | 60.5 | 46.5 |
| 11 | 416 | 416 | 382 | 382 | 404 | 404 | 601 | 601 | ||
| 12 | 4.0 | 3.9 | 65.0 | 56.1 | 72.0 | 65.2 | 67.9 | 54.9 | 68.1 | 59.3 |
| 12 | 277 | 277 | 263 | 263 | 282 | 282 | 367 | 367 | ||
| 13 | 3.9 | 3.7 | 67.7 | 56.8 | 71.7 | 62.4 | 67.1 | 52.8 | 71.2 | 60.8 |
| 13 | 411 | 411 | 374 | 374 | 393 | 393 | 513 | 513 | ||
|
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| 14 | 3.7 | 3.6 | 78.3 | 73.7 | 79.8 | 79.9 | 78.5 | 76.3 | 80.6 | 83.1 |
| 14 | 296 | 296 | 279 | 279 | 293 | 293 | 365 | 365 | ||
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| 15 | 3.6 | 3.5 | 87.0 | 79.5 | 95.7 | 87.3 | 82.7 | 67.2 | 87.6 | 81.3 |
| 15 | 243 | 243 | 243 | 243 | 240 | 240 | 309 | 309 | ||
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| 16 | 3.5 | 3.4 | 83.5 | 76.1 | 90.4 | 92.7 | 87.6 | 88.8 | 87.6 | 89.8 |
| 16 | 286 | 286 | 283 | 283 | 295 | 295 | 358 | 358 | ||
|
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| 17 | 3.4 | 3.3 | 91.1 | 91.5 | 93.2 | 88.0 | 90.1 | 89.0 | 94.8 | 98.4 |
| 17 | 275 | 275 | 262 | 262 | 271 | 271 | 338 | 338 | ||
| 18 | 3.3 | 3.2 | 92.6 | 95.7 | 90.5 | 84.9 | 88.8 | 90.0 | 90.5 | 89.4 |
| 18 | 247 | 247 | 228 | 228 | 253 | 253 | 303 | 303 | ||
|
| ||||||||||
| Overall: Phase residual | 49.469 | 47.539 | 48.459 | 48.493 | ||||||
| Number of spots | 7320 | 7071 | 7267 | 10385 | ||||||