Table 1.
MRM settings. The specific MRM settings for each ion are presented in the table. The specific tuning parameters for the MS/MS (Sciex API 4000) were ion source temperature 550 °C, ion source voltage +5500 V, nebulizer gas setting 50, drying gas setting 60, curtain gas setting 20, entrance potential +10 V and nitrogen collision chamber gas pressure 6 psi
| Q1 | Q3 | Dwell (ms) | DP | CE | CXP |
|---|---|---|---|---|---|
| 380.3 | 264.5 | 200 | 81 | 27 | 16 |
| 380.3 | 82.1 | 200 | 81 | 45 | 14 |
| 387.3 | 271.1 | 200 | 91 | 27 | 14 |
| 387.3 | 82.1 | 200 | 91 | 47 | 8 |
| 763.6 | 185.3 | 30 | 110 | 43 | 12 |