Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C23H22FN5S |
| M r | 419.51 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 297 |
| a, b, c () | 6.4388(8), 23.482(3), 14.572(3) |
| () | 100.5009(19) |
| V (3) | 2166.3(6) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.18 |
| Crystal size (mm) | 0.40 0.27 0.09 |
| Data collection | |
| Diffractometer | Bruker APEXII DUO CCD area-detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2009 ▸) |
| T min, T max | 0.779, 0.932 |
| No. of measured, independent and observed [I > 2(I)] reflections | 24228, 5094, 3393 |
| R int | 0.041 |
| (sin /)max (1) | 0.657 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.046, 0.127, 1.04 |
| No. of reflections | 5094 |
| No. of parameters | 278 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 0.24, 0.19 |