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. 2015 Oct 17;71(Pt 11):o860–o861. doi: 10.1107/S2056989015019325
Bruker X8 Proteum diffractometer 2371 independent reflections
Radiation source: Bruker MicroStar microfocus rotating anode 2225 reflections with I > 2σ(I)
Helios multilayer optics monochromator Rint = 0.040
Detector resolution: 18.4 pixels mm-1 θmax = 64.1°, θmin = 5.6°
φ and ω scans h = −7→6
Absorption correction: multi-scan (SADABS; Bruker, 2013) k = −15→15
Tmin = 0.786, Tmax = 0.838 l = −18→18
6729 measured reflections