| Crystal data |
| Chemical formula |
[Ni(C48H60N4O2)] |
|
M
r
|
783.71 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
11.9496(6), 13.6692(6), 14.3909(7) |
| , , () |
72.018(2), 69.051(2), 89.558(2) |
|
V (3) |
2074.03(17) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.51 |
| Crystal size (mm) |
0.30 0.14 0.03 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEXII area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2014 ▸) |
|
T
min, T
max
|
0.704, 0.745 |
| No. of measured, independent and observed [I > 2(I)] reflections |
50235, 7609, 4733 |
|
R
int
|
0.103 |
| (sin /)max (1) |
0.603 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.044, 0.088, 0.92 |
| No. of reflections |
7609 |
| No. of parameters |
525 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.85, 0.73 |
