| Bruker SMART CCD area-detector diffractometer | 2374 independent reflections |
| Radiation source: fine-focus sealed tube | 2172 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.061 |
| ω scans | θmax = 27.5°, θmin = 2.1° |
| Absorption correction: analytical (SADABS; Bruker, 1998) | h = −12→10 |
| Tmin = 0.340, Tmax = 0.503 | k = −18→18 |
| 6331 measured reflections | l = −8→9 |
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