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| [Bi2Cl10](C6H14N2)22H2O | [Sb2Cl10](C6H14N2)22H2O | Parameter variation (%) [(X Bi X Sb)/(X Sb)]100 | |
|---|---|---|---|
| Crystal system | monoclinic | orthorhombic | - |
| Space group | P21/c | Pnnm Pnmn (cba) | - |
| a () | 7.875(3) | 9.162(1) => 7.566(2) | 4.08(2) |
| b () | 18.379(5) | 20.689(7) => 20.689(7) | 11.16(3) |
| c () | 10.444(4) | 7.566(2) => 9.162(1) | 13.99(2) |
| () | 105.95(3) | 90.00 | - |
| V (3) | 1453.4(9) | 1446.8(7) | 0.45(7) |
