Table 4. Experimental details.
| Crystal data | |
| Chemical formula | (C6H14N2)2[Bi2Cl10]2H2O |
| M r | 1036.88 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 293 |
| a, b, c () | 7.875(3), 18.379(5), 10.444(4) |
| () | 105.95(3) |
| V (3) | 1453.4(9) |
| Z | 2 |
| Radiation type | Mo K |
| (mm1) | 13.03 |
| Crystal size (mm) | 0.5 0.3 0.2 |
| Data collection | |
| Diffractometer | EnrafNonius CAD-4 |
| Absorption correction | scan (North et al., 1968 ▸) |
| T min, T max | 0.013, 0.074 |
| No. of measured, independent and observed [I > 2(I)] reflections | 3159, 3159, 2681 |
| R int | 0.035 |
| (sin /)max (1) | 0.638 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.036, 0.102, 1.06 |
| No. of reflections | 3159 |
| No. of parameters | 142 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 3.48, 2.57 |