| Crystal data |
| Chemical formula |
C21H33N3O3
|
|
M
r
|
375.50 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
9.7020(2), 10.1456(3), 11.2064(3) |
| , , () |
96.528(2), 95.982(2), 112.110(2) |
|
V (3) |
1002.30(5) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.08 |
| Crystal size (mm) |
0.47 0.24 0.10 |
| |
| Data collection |
| Diffractometer |
Agilent SuperNova, Eos |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
|
T
min, T
max
|
0.657, 1 |
| No. of measured, independent and observed [I > 2(I)] reflections |
24791, 4106, 3603 |
|
R
int
|
0.027 |
| (sin /)max (1) |
0.625 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.052, 0.142, 1.04 |
| No. of reflections |
4106 |
| No. of parameters |
244 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.61, 0.21 |
